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Separative chemistry at DiSC is performed on a wide range of chromatography equipment, ranging from gas phase carrier systems to liquid to gel.
Facilities for gas chromatography are available, including: (i) apolar, medium polar, polar columns for liquid samples; (ii) fast-GC equipped with; (iii) GC-MS analysis; (iv) instruments for gas analysis, equipped with FID/TCD/MS detector.
Thermo Scientific DSQ™ single quadrupole GC/MS systems
GC-MS: Thermo Scientific trace GC ultra with DSQ quadrupole mass analyzer and XPT purge and trap sample concentrator. Thermo Scientific DSQ™ single quadrupole GC/MS systems take trace level analysis into the future by providing innovation and performance while ensuring reliable, accurate analytical results.
GC/MS Agilent 6850
GC/MS Agilent 6850 with 5973 Network Mass Selective Detector.
FAST GAS CROMATOGRAPHY Shimadzu GC-2010
The Shimadzu GC-2010 with hydrogen generator is a fast gas chromatographic system equipped with AOC-20i autoinjector. It represents the evolution of GC, allowing to work with 5 atm pressures on ad hoc developed columns. The system is interfaced to a CLAIMO Hydrogen Generator.
Agilent Technologies 5975C VL MSD 7890A GC system triple-axis detector
Gas Chromatograph characterized by a quadrupolar mass separation system, equipped with triple axis detector, FID & TCD.
VARIAN 430 GC with autosampler
Gas chromatograph equipped with powerful autosampler, working 24h/day.
hp6890 GC system Plus+
Shimadzu GC 14B
HPLC Dionex with P680 pump, thermostated column compartment, TCC-100 and PDA-100 photodiode array detector, ASE 100: accelerated solvent extractor.
VWR Hitachi Chromaster HPLC
The Chromaster HPLC is an analytical system, equipped with a 5160 pump, a 5260 autosampler and a 5410 UV detector. The main feature of the system is the high reproducibility of the gradient and retention times, achieved thanks to a low pressure operating mode, called the High Frequent Mode (HFM), which is based on the double switching function of proportioning valves. The autosampler compartment is equipped with a high precision syringe drive unit, for high accuracy and volume reproducibility. Substantially there's no dead volume in the flow path, thanks to a pumping method that washes the needle outer wall. The equipment is actually dedicated to the analysis of the synthesized peptides purity.
Agilent Technologies HPLC 1200 series
This HPLC is equipped with manual injection and diode array, VWD + Bin Pump. It is actually mostly dedicated to the determination of the analytical purity of synthesized peptides and proteins. A senior technical staff is dedicated to students training for the instruments best application as well as research and industry collaborations.
HPLC Shimadtzu single-pump system for isocratic separations
The equipment is composed of a LC-10AD liquid chromatography pumping unit, a degassing unit and a SPD-10A UV-Vis detector.
Twin set of HPLC Shimadzu systems for gradient elution separations
Each system is composed by two LC-10AT liquid chromatography pumping units and one SPD-10A UV-Vis detector. They are dedicated to direct phase and inverse phase chromatographic analyses.
HPLC Thermoquest (TSP) for gradient elution separations
The analytical liquid chromatography system is composed by a P2000 TSP pumping unit, a degasser and a UV6000LP diode-array detector.
Pharmacia Biotech P900 with UV-900
Agilent Technologies 1260 Infinity
The equipment include the 1260 Iso Pump, 1260 TCC, the Agilent 1260 Infinity Variable Wavelength Detector (VWD) VL, the 1260 Infinity Refractive Index Detector (RID, 1260 Infinity Thermostatted Column Compartment and 1260 manual injection system. For routine polymer characterization by GPC/SEC separation with refractive index or UV-Vis detectors. It has a high flow precision (600 bar power range and up to 10 mL/min) and temperature stability from 10° below room temperature to 80°C. The GPC/SEC software allows instrument control, collection of multiple data channels and performs all standard molecular weight and branching calculations. The instrument is mainly used for GPC/SEC separations in organic solvents.
Portlab Ion chromatography
Ion chromatography is performed by a Portlab HPLC SYSTEM STAYER equipped with a thermostated cell compartment and a CD-516 conductivity detector.
HPLC Shimadzu CT10-10ASVP column oven equipped with autosampler
The system is composed by the CTO-10AS column oven compartment, the DGU-14A module, the LC-10AD liquid chromatograph unit, the FCV-10AL module, the SIL-10AD auto injector system, the SPD-10AV UV-Vis detector, the SCL-10A system controller.
Protein Purification systems AKTApurifier
HPLC Shimadzu (1990) for preparative separations
Biotage IsoleraTM Prime (two of them)
Shimadzu Preparative HPLC with SPD-6A UV detector
Preparative chromatography Sepacore